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The long, straight grain boundary of the high-entropy alloy (HEA) produced via laser melting deposition (LMD) is prone to cracking due to unidirectional scanning (single wall). To enhance the competitive growth of columnar grains and improve the overall performance of the alloy, a vertical cross scanning method was employed to fabricate FeCoCrNi HEA (bulk). The influence of grain orientation on the microstructure and mechanical properties of FeCoCrNi-LMD was systematically investigated. Microhardness tests and tensile tests were conducted to assess the mechanical property differences between the single-wall and bulk samples. This study shows that using a single scanning strategy results in monolayer wall grains sized at 129.40 μm, with a max texture strength of 21.29. Employing orthogonal scanning yields 61.15 μm block-like grains with a max texture strength of 11.12. Dislocation densities are 1.084 × 1012 m−2 and 1.156 × 1012 m−2, with average Schmid factors of 0.471 and 0.416 ....
Investigating the catalytic behavior of the liquid fuels on well-defined dual sites is crucial in understanding electrocatalytic reactions. Herein, concept holding bidirectional electronegativity dominant d-band center regulation on Pt-Rh dual sites is proposed to tailor the catalytic behaviors toward methanol oxidation reaction (MOR). The Pt-Rh dual sites are engineered by introducing the low-electronegativity Ga/Ni and high-electronegativity W elements in PtRhGaNiW high-entropy alloy (HEA), which can drive the electron cloud of Pt-Rh dual sites redispersing over a wide orbit window. The optimized Pt-Rh dual sites in PtRhGaNiW HEA nanowire achieve a high current density of 5.61 mA cm−2 toward MOR, which is 3.38 and 9.75 times than that of PtRh alloy (1.66 mA cm−2) and Pt/C (0.57 mA cm−2), as well as remarkably stability and COads poisonous resistance. The theoretical calculations further disclose that the redistribution of surface localized electron around Pt-Rh dual sites can p ....
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A functionally graded AlxCoCrFeNi high entropy alloy with a variation in Al concentration along the building direction was in-situ produced using a hybrid powder-bed wire-based direct energy deposition process. A continuous transition from a single FCC structure to a major BCC+minor FCC dual-phase structure was achieved, benefiting from the remelting and reheating process during the deposition. In the FCC→BCC transition zone, the dendritic core region is identified as an FCC matrix decorated by AlNi-rich ordered B2 precipitates. The interdendritic area shows B2 precipitating in the FeCr-rich disordered A2 matrix. Additionally, the interface between the two regions shows that the A2 phase and ordered Cr3Fe intermetallic phase precipitate at the B2 phase. The mechanical properties show a tendency for higher strength and hardening rate but lower plasticity corresponding to the areas with higher Al content. Through quantitative estimation of different strengthening mechanisms, the contri ....