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Luis Gustavo , Good Morning , Half Maximum , லூயிஸ் குஸ்டாவோ , நல்ல காலை , பாதி அதிகபட்சம் ,

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kathimerini.com.cy - get the latest breaking news, showbiz & celebrity photos, sport news & rumours, viral videos and top stories from kathimerini.com.cy Daily Mail and Mail on Sunday newspapers.

Luis Gustavo , Good Morning , Half Maximum , லூயிஸ் குஸ்டாவோ , நல்ல காலை , பாதி அதிகபட்சம் ,

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kathimerini.com.cy - get the latest breaking news, showbiz & celebrity photos, sport news & rumours, viral videos and top stories from kathimerini.com.cy Daily Mail and Mail on Sunday newspapers.

Luis Gustavo , Good Morning , Half Maximum , லூயிஸ் குஸ்டாவோ , நல்ல காலை , பாதி அதிகபட்சம் ,

Solid-state NMR of unlabeled plant cell walls: high-resolution structural analysis without isotopic enrichment

Background
Multidimensional solid-state nuclear magnetic resonance (ssNMR) spectroscopy has emerged as an indispensable technique for resolving polymer structure and intermolecular packing in primary and secondary plant cell walls. Isotope (
13C) enrichment provides feasible sensitivity for measuring 2D/3D correlation spectra, but this time-consuming procedure and its associated expenses have restricted the application of ssNMR in lignocellulose analysis.
Results
Here, we present a method that relies on the sensitivity-enhancing technique Dynamic Nuclear Polarization (DNP) to eliminate the need for
13C-labeling. With a 26-fold sensitivity enhancement, a series of 2D
13C–
13C correlation spectra were successfully collected using the unlabeled stems of wild-type ....

Sensitivity Enhancement , Full Width , Half Maximum , உணர்திறன் விரிவாக்கம் , முழு அகலம் , பாதி அதிகபட்சம் ,