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What is Fe3O4?Exceptional magnetic properties of magnetite, Fe3O4, and nanoparticles make them one of the most intensively studied inorganic nanomaterials for biomedical applications. We report successful gram-scale syntheses of colloidal Fe3O4 nanoparticles with sizes of 12.9 ± 5.9, 17.9 ± 4.4, and 19.8 ± 3.2 nm via hydrothermal route or controlled coprecipitation in an automated reactor. To investigate structure−property relationships as a function of the synthetic procedure, we used multiple ....