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she suspected in march at which time she followed her instincts and contacted the police. reporter: for five months lisa hill lived in fear in the couple s home as investigators secretly took samples of the coffee her husband delivered to her bedside every morning. when the test results came back they were shocking, extreme levels of barium in her coffee, a toxic heavy metal that is poisonous and causes flu-like symptoms. when we got the lab results back, nobody was more surprised than lisa that her fear had been confirmed. and that it was actually possible that her husband was trying to do her great harm. reporter: the police told her her previous health issues are consistent with heavy metal poisoning. they tell us no charges have been filed at this point, but her husband is not allowed near their home. this is and will be a continuing and slow, methodical investigation. reporter: if this is a case of spousal poisoning it won t be the first. in 2005, nancy kissel was convic

Heavy metalTest resultsLab resultsNancy kisselHeavy metal poisoning